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This document specifies a method for the determination of the time-weighted average mass concentration of hydrogen chloride (HCl) gas and hydrochloric acid mist, hydrogen bromide (HBr) vapour and hydrobromic acid mist and nitric acid (HNO3) vapour and mist in workplace air by collection on an alkali-impregnated quartz fibre filter and analysis by ion chromatography.
For mist sampling, the method is applicable to the personal sampling of the inhalable fraction of airborne particles, as defined in ISO 7708, and to static (area) sampling.
The procedure is intended to differentiate between the acids and their corresponding salts. If both are present in the air, particulate salts are trapped on a pre-filter. Co-sampled particulate matter trapped on the pre-filter and/or deposited on the walls of the sampler can be analysed, if desired.
Acids can react with co-sampled particulate matter on the pre-filter, causing interference with the measurement of the acid concentration.
This document specifies a method for the determination of sulfur dioxide (SO2) in flue gas of stationary sources and describes the fundamental structure and the key performance characteristics of automated
measuring systems.
The method allows continuous monitoring with permanently installed measuring systems of SO2 emissions.
This document describes extractive systems and in situ (non-extractive) systems in connection with a range of analysers that operate using, for example, the following principles:
— non-dispersive infrared absorption (NDIR);
— Fourier transform infrared (FTIR) spectroscopy;
— laser spectroscopic technique or tunable laser spectroscopy (TLS);
— non-dispersive ultraviolet absorption (NDUV);
— differential optical absorption spectroscopy (DOAS);
Other equivalent instrumental methods can be used provided they meet the minimum performance requirements specified in this document. The measuring system can be validated with reference materials, in accordance with this document, or comparable methods.
Automated measuring system (AMS) based on the principles listed above has been used successfully in this application for the measuring ranges as shown in (Annex E).